白姐资料二四六精选

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氟化石墨合成方法与分析方法

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氟化石墨合成方法与分析方法

发布日期:2019-12-06 00:00 来源:http://qyforum.com 点击:

白姐资料二四六精选FUHUASHIMOHECHENGFANGFAYUFENXIFANGFA

“GF”DEHECHENGFANGFAHENDUO,DANBUWAIHUSHIGANFAHESHIFAERZHONG。GANFASHIZAIDUOXINGQITIZHONGJIANGSHIMOHEFUTONGGUODUOXIANGJIECHUERZHIDE。ZHEISHIJIAOWEICHANGYONGDEFANGFA。SHIFAJIDIANJIEFA,QIGONGYIGUOCHENGJIBENHESUANHUASHIMODIANJIEYANGHUAFAXIANGTONG,DANSHIFAJIAOSUANHUASHIMOHECHENGFAFUZADEDUO,RUWENDU、YALI、GONGQILIANG、YUANLIAOZHONGLEIDENGYAOQIUJIAOGAO,CIWAI,SHANGYOUFANGBAO、FANGDUHEFANGFUDENGWENTI。

1、GANSHIHECHENGFA:GANFADESHIZHISHIJIANGSHIMOYUFUZHIJIEJIECHUFANYINGERZHIDE。FANYINGWENDUYIBANWEI320~6500C,YALIWEI1~5GEDAQIYA,QIHECHENGZHUANGZHI:FANYINGQIYOUWAIQIAO、HUOGAI、FANYINGSHI、JINQIGUAN、PAIQIZHUANGZHI、TOUQISHENGLIAOZHUANGZHI、WANGSHIJIAREZHUANGZHI、SHIMO、JIACHIHUAN、KEXIEKONGXIANG、GERECENG、WENDUCHUANGANQIDENGZUCHENG。FANSHIHEFUJIECHUBUFENQUANBUYONGJINSHUNIEZHIZAO,QITAZHUANGZHISHANGYOU:ZHILINGJIGOU、DIAOJIEQI、LIULIANGJIWEIFUHEDUOXINGQITI。QITIDIAOJIEZHUANGZHIHEFANYINGSHIDEJINQIGUANXIANGLIAN,BINGHEHUNHEJIGOUXIANGTONG。PAIQIBUFENJINJIEFEIQIJINGHUAZHUANGZHI。

合成进程如下:将带隔热层的外壳上取下活盖、箱、夹持环,压紧网,在筛网上放入石墨,石墨化焦再按程序将反应室装好,打开进气管使惰性气体进入反应室,当传感器显示工作温度正常时,指令结构接通氟的通气管开始供气,在流量计的显示下,气体依次通过混合器,进气管,透气装置,石墨,反应器,排气管和净化装置,借助加热装置的功率调节器使反应室保持规定的温度,氟化完毕,加热装置自动切断电源,并减少氟的供应量,待氟化产物冷却到规定的温度后,惰性气体进气装置自动停止供气,最后按加料程序取出氟化石墨,检验分析。

白姐资料二四六精选YINGXIANGFUHUADEYINSU:(1)FANYINGQIDEGOUZAO:FANYINGQIZHILIANGDEYOULIE,ZHIJIEYINGXIANGFUHUAXIAOGUOYUCHANLV,CHANLIANGYIJIANQUANSHENGCHANDENGFANGMIAN。YOURENJIANYIJIANGSHIMOFANGZAIYIGEZHENDONGZHUANGZHISHANG,TONGGUOBUDUANDEZHENDONGSHISHIMOKUANGYUFUJIECHU,YITIGAOFANYINGXIAOLV,DANZHEIZHONGZHUANGZHIJIAOWEIFUZA。DIERZHONGSHICAIYONGLIUTAIHUAFUHUA,CONGFANYINGXIAOLVLAIKANZHEIZHONGZHUANGZHIJIAOLIXIANG,DANCAOZUODIAOJIEHEFANGDUDOUCUNZAIWENTI。QIANSULIANCENGSHEJIYIZHONGLISHIFUHUALU。GAIFUHUALUDEGONGZUOYUANLIHEYIBANFUHUALUXIANGTONG,JUCHENGFUHUAXIAOGUOJIAOHAO。


石墨化焦

白姐资料二四六精选(2)YUANLIAODEZHONGLEIHETEXING:HECHENGFUHUASHIMODEYUANCAILIAOZHUYAOSHISHIMO、FUHEDUOXINGQITI。SHIMODEZHONGLEI、LIDU、CHUNDUHEJINGTIHUACHENGDUDOUDUIFUHUAGUOCHENGYOUJIAODADEYINGXIANG。FUHUASHIMODEYUANLIAOKEYISHITIANRANLINPIANSHIMO,YEKEYICAIYONGREJIESHIMO、RENZAOSHIMO、TANXIANWEI、JIAOTANYIJITANHEIDENG。SHIMOHUAJIAOBUTONGDEYUANLIAOQIFUHUAWENDU、SUDUJICHANLVDOUBUYIYANG。DANGCAIYONGTIANRANSHIMOSHI,FANYINGWENDUDAYU5000C,ZECHANLVXIAJIANG,RUFANYINGWENDUXIAOYU3000CZECHANLVYEXIAJIANG,DANZAICHANLVXIAJIANGDEWENDUFANWEINEI,YOUYUFANYINGWUDEFENJIEHEZAIYANGHUA,CHANPINJIEJINGCHENGDUYOUSUOGAISHAN。

(3)FANYINGTIAOJIAN:FANYINGTIAOJIANZHUYAOZHIFANYINGWENDU、YALI、SHIJIAN。FANYINGWENDUQUJUEYUCAILIAODELEIXINGHECHANWUCHENGFEN,FANYINGWENDUDI,ZEFANYINGSULVMAN,WENDUGUOGAOZECHANWURONGYIFENJIE,CHANLVYEXIANGYINGJIANGDI,BINGCHANSHENGYOUDUQITI,YIBANFANYINGWENDUZAI300~6000CZHIJIAN,ZAICIWENDUFANWEINEIKEYIDEDAOWENDINGDE(CF)nJI(C2F)n。

ANQUANZHIQUFUHUASHIMODEFANGFA:FUHUASHIMODEHECHENGFANGFAYIBANDOUSHICAIYONGJIECHUFA,JIJIANGSHIMOJIAREDAOYIDINGWENDU,RANHOUJIANGQIYUFUJIDUOXINGQITIZHIJIEJIECHUERZHIDE,ZHEIZHONGFANGFADEQUEDIANSHIFUYOUDU,DUIRENJIZHOUWEIHUANJINGDOUYOUBULIANGYINGXIANG,QICISHIFUDEHUAXUEXINGZHIJIWEIHUOPO,FUSHIXINGHENQIANG,YINCI,SHEBEIFANGFUSHIGEWENTI,DISANSHIFANYINGWENDUJIAOGAO,YOUBAOZHAWEIXIAN,YANJIUZHEXIWANGYOUYIZHONGBUYONGFUQIDEANQUANHECHENGFA。ANQUANHECHENGDESHIZHISHIBAHANFUDEJUHEWUHETANZAIDUOXINGQITICUNZAIXIAJINXINGHECHENG“(GF)”。FANYINGWENDUYIBANWEI350~5000C。HANFUHUAHEWUYIBANCAIYONGSIFUYIXI、LIUFUYIXI,LVSANFUYIXIDENG。TANCAILIAOWEISHIMO、TANHEI、SHIYOUJIAO、MUTANJITANXIANWEIDENGTANSUCAILIAO。LIDUWEI50~10μYIXIA,YIXIWEIHAO。F/CZHIBIZHIGENJUYUANLIAOZHONGLEI,FANYINGWENDUHESHIJIANYIJISHIYONGMUDEERDING。DUOXINGQITIYIDANHUOYAWEIZUILIXIANG。FANYINGSHIJIANCONGJIFENZHONGDAOJIXIAOSHI,YALIWEI1~5GEDAQIYA。

白姐资料二四六精选2、SHIFA:YOUYUGANFAHENNANLIANXUZUOYE,DAGUIMOSHENGCHANSHOUDAOXIANZHI。YANJIUZHECHANGYILEDIANJIEFA。DIANJIEFAYISHIMOWEIYANGJI,FUQINGSUANWEIYINJI,QIZHUANGZHIWEIYANGJI、YINJI、XUNHUANBENG、BANTOUMO、QITIYICHUKONG、DIANYUAN,FUQINGSUANKETONGGUOBANTOUMO,DANSHIMOKELIBUNENGTONGGUO,GAIZHUANGZHIKELIANXUSHENGCHAN。


相关标签:石墨化焦

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